方法:采用高效液相色谱法,对栀子中栀子苷的含量进行测定。
结论:柱层析和重结晶方法是简单、快速分离栀子苷的有效办法。
结论D301R型大孔树脂用作栀子苷的分离效果较好。
1·Conclusion: Silica gel column chromatography and crystallization are simple and rapid methods to isolate gardenoside.
结论:柱层析和重结晶方法是简单、速分离栀子苷的有效办法。
2·Results Under the optimum process condition of flocculation impurity removal, gardenoside contents in the flocculation group is higher than those in 50% , 75% alcohol groups.
结果采用优化后的絮凝除杂工艺条件,絮凝组中栀子苷含量明显高于50%、75%乙醇醇沉组;
3·Methods: Silica gel column chromatography and crystallization were used to obtained gardenoside from Gardenia jasminoides.
方法:利用柱层析、结晶从山栀子的成熟果实中进行分离纯化栀子苷。
1·Object To optimize the macroporous resin for separating gardenoside.
目的优选分离栀子苷的大孔树脂。